Please use this identifier to cite or link to this item: https://hdl.handle.net/11681/43964
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dc.contributor.authorGibbons, Stephen-
dc.contributor.authorKennedy, Alan James, 1976--
dc.contributor.authorKremer, Kathryn-
dc.contributor.authorWu, Qihua-
dc.creatorEnvironmental Laboratory (U.S.)-
dc.date.accessioned2022-04-15T16:01:07Z-
dc.date.available2022-04-15T16:01:07Z-
dc.date.issued2022-04-
dc.identifier.govdocERDC/EL SR-22-1-
dc.identifier.urihttps://hdl.handle.net/11681/43964-
dc.identifier.urihttp://dx.doi.org/10.21079/11681/43964-
dc.descriptionSpecial Reporten_US
dc.description.abstractRheology studies the flow of matter and is one of the most important methods for materials characterization because flow behavior is responsive to properties such as molecular weight and molecular weight distribution. Rheological properties help practitioners understand fluid flow and how to improve manufacturing processes. Rheometers have been extensively used to determine the viscosity and rheological properties of different materials because the measurements are quick, accurate, and reliable. In this standard operating procedure, a general protocol using a rotational rheometer is developed for characterizing rheological properties of nanomaterials. Procedures and recommendations for sample preparation, instrument preparation, sample measurements, and results analysis are included. The procedure was tested on a variety of carbon-based nanomaterials.en_US
dc.description.sponsorshipUnited States. Army. Corps of Engineers.en_US
dc.description.tableofcontentsAbstract ............................................................................................................................................................. ii Figures and Tables .............................................................................................................................................. iv Preface ................................................................................................................................................................ v 1 Introduction ................................................................................................................................................ 1 Background ................................................................................................................................. 1 Objectives ................................................................................................................................... 2 Scope ......................................................................................................................................... 2 2 Terminology ................................................................................................................................................ 3 Related documents ...................................................................................................................... 3 Definitions ................................................................................................................................... 3 3 Materials and Apparatus ............................................................................................................................. 4 Materials ..................................................................................................................................... 4 Apparatus.................................................................................................................................... 4 4 Procedure ................................................................................................................................................... 5 Experiment preparation ................................................................................................................ 5 Sample preparation .................................................................................................................................... 5 Instrument preparation................................................................................................................................ 5 Sample analysis ........................................................................................................................... 6 Start-up 6 Instrument parameters ................................................................................................................................ 7 Perform measurement ................................................................................................................................. 8 Shut-down ................................................................................................................................................. 9 5 Reporting ................................................................................................................................................. 10 Analysis of results....................................................................................................................... 10 QA/QC Considerations ............................................................................................................... 11 6 Summary..................................................................................................................................................12 References .......................................................................................................................................................13 Report Documentation Page-
dc.format.extent21 pages / 1.37 MB-
dc.format.mediumPDF-
dc.language.isoen_USen_US
dc.publisherEngineer Research and Development Center (U.S.)en_US
dc.relation.ispartofseriesSpecial Report (Engineer Research and Development Center (U.S.)) ; no. ERDC/EL SR-22-1-
dc.rightsApproved for Public Release; Distribution is Unlimited-
dc.sourceThis Digital Resource was created in Microsoft Word and Adobe Acrobat-
dc.subjectRheologyen_US
dc.subjectMaterials--Testingen_US
dc.subjectCarbonen_US
dc.subjectViscosity--Measurementen_US
dc.subjectNanostructured materialsen_US
dc.titleDetermination of nanomaterial viscosity and rheology properties using a rotational rheometeren_US
dc.typeReporten_US
Appears in Collections:Special Report

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