Please use this identifier to cite or link to this item:
https://hdl.handle.net/11681/12056
Title: | Analytical methods for determining nitroguanidine in soil and water |
Authors: | U.S. Toxic and Hazardous Materials Agency Walsh, Marianne E. |
Keywords: | Analytical methods Munitions Explosives Nitroguanidine Groundwater pollution Pollution |
Publisher: | Cold Regions Research and Engineering Laboratory (U.S.) Engineer Research and Development Center (U.S.) |
Series/Report no.: | Special report (Cold Regions Research and Engineering Laboratory (U.S.)) ; 89-35. |
Description: | Special Report Abstract: Methods were developed for determining nitroguanidine in soil and water. The soil method involves extracting a 2-g sample with water using an ultrasonic bath. Soil extracts and water samples are filtered through a 45-~membrane prior to determination by RP-HPLC. Separations are achieved on a mixed-mode RP18/cation column eluted with 1.5 mL/min of water; detection is by UV (~ = 263 nm). Certified reporting limits were estimated at 5.0 ~g/L for water and 0.5 ~g/L for soil. Note: Certain scientific symbols could not be rendered by the character set available to this program, a ~ has been inserted to indicated missing symbols. The file contains the symbols in question. |
Rights: | Approved for Public Release, Distribution is Unlimited |
URI: | http://hdl.handle.net/11681/12056 |
Appears in Collections: | Special Report |
Files in This Item:
File | Description | Size | Format | |
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SR-89-35.pdf | 1.46 MB | Adobe PDF | ![]() View/Open |