Please use this identifier to cite or link to this item: https://hdl.handle.net/11681/11806
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dc.contributorU.S. Army Environmental Center-
dc.contributor.authorHewitt, Alan D. (Alan Dole)-
dc.date.accessioned2016-06-20T14:25:22Z-
dc.date.available2016-06-20T14:25:22Z-
dc.date.issued1999-05-
dc.identifier.urihttp://hdl.handle.net/11681/11806-
dc.descriptionSpecial Report-
dc.descriptionAbstract: Traditionally, soil samples obtained for characterizing or monitoring sites for volatile organic compounds (VOCs) have been transported off site before initiating the preparation steps necessary for analysis. In the most recent regulatory guidance, only a two-day holding period at 4 ± 2°C is recommended before a sample should be preserved, so as to allow storage up to 14 days prior to instrumental analysis. The transportation and storage of soil samples were evaluated for (1) covered core barrel liners, (2) En Core samplers, and (3) empty volatile organic analysis (VOA) vials under different conditions. Core barrel liners covered with either of two formulations of Teflon sheeting or aluminum foil failed to prevent rapid losses of VOCs. En Core samplers and otherwise empty VOA vials were suitable transportation and storage chambers for samples. These chambers not only meet the initial requirement to retain VOCs for two days when held at 4 ± 2°C for transportation purposes, but frequently showed no significant loss of VOCs after placing in a freezer and storing at –12 ± 3°C for an additional 12 days.-
dc.publisherCold Regions Research and Engineering Laboratory (U.S.)-
dc.publisherEngineer Research and Development Center (U.S.)-
dc.relationhttp://acwc.sdp.sirsi.net/client/en_US/search/asset/1001505-
dc.relation.ispartofseriesSpecial report (Cold Regions Research and Engineering Laboratory (U.S.)) ; 99-5.-
dc.rightsApproved for public release; distribution is unlimited.-
dc.sourceThis Digital Resource was created in Microsoft Word and Adobe Acrobat-
dc.subjectPreservation-
dc.subjectVolatile organic compounds-
dc.subjectSoil samples-
dc.subjectSoils-
dc.subjectStorage-
dc.subjectSampling-
dc.titleStorage and preservation of soil samples for volatile compound analysis-
dc.typeReporten_US
Appears in Collections:Special Report

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